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Information card for entry 1545975
Preview
Coordinates | 1545975.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C8 H14 B O3 P |
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Calculated formula | C8 H14 B O3 P |
SMILES | [P@]12([BH3])O[C@H](C=C)C[C@H](O1)C=CCO2 |
Title of publication | P-Stereogenic Bicyclo[4.3.1]phosphite Boranes: Synthesis and Utility of Tunable P-Tether Systems for the Desymmetrization of C2-Symmetric 1,3-anti-Diols. |
Authors of publication | Markley, Jana L.; Hanson, Paul R. |
Journal of publication | Organic letters |
Year of publication | 2017 |
Journal volume | 19 |
Journal issue | 10 |
Pages of publication | 2552 - 2555 |
a | 6.2929 ± 0.001 Å |
b | 11.2901 ± 0.0017 Å |
c | 14.454 ± 0.002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1026.9 ± 0.3 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0267 |
Residual factor for significantly intense reflections | 0.0267 |
Weighted residual factors for significantly intense reflections | 0.0701 |
Weighted residual factors for all reflections included in the refinement | 0.0701 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.078 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1545975.html
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