Information card for entry 1546414

Structure parameters

• Formula: C236 H503 Dy52 N53 Ni52 O407
• Calculated formula: C236 H283 Dy52 N53 Ni52 O407
• Title of publication: Lantern-shaped 3d–4f high-nuclearity clusters with magnetocaloric effect
• Authors of publication: Lin, Qingfang; Li, Jing; Dong, Yayu; Zhou, Guangpeng; Song, You; Xu, Yan
• Journal of publication: Dalton Transactions
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 30
• Pages of publication: 9745 - 9749
• a: 28.62 ± 0.003 Å
• b: 41.352 ± 0.004 Å
• c: 29.564 ± 0.003 Å
• α: 90°
• β: 108.087 ± 0.001°
• γ: 90°
• Cell volume: 33260 ± 6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1259
• Residual factor for significantly intense reflections: 0.0737
• Weighted residual factors for significantly intense reflections: 0.2128
• Weighted residual factors for all reflections included in the refinement: 0.2421
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No