Information card for entry 1546464

Structure parameters

• Formula: C13 H27 F2 N O Si
• Calculated formula: C13 H27 F2 N O Si
• SMILES: [Si](C(F)(F)CCC(=O)N(C(C)C)C(C)C)(C)(C)C
• Title of publication: Radical Silyldifluoromethylation of Electron-Deficient Alkenes.
• Authors of publication: Supranovich, Vyacheslav I.; Levin, Vitalij V.; Struchkova, Marina I.; Korlyukov, Alexander A.; Dilman, Alexander D.
• Journal of publication: Organic letters
• Year of publication: 2017
• Journal volume: 19
• Journal issue: 12
• Pages of publication: 3215 - 3218
• a: 11.8766 ± 0.0006 Å
• b: 11.7308 ± 0.0006 Å
• c: 23.6382 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3293.3 ± 0.3 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0537
• Residual factor for significantly intense reflections: 0.0396
• Weighted residual factors for significantly intense reflections: 0.092
• Weighted residual factors for all reflections included in the refinement: 0.1025
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No