Information card for entry 1546503

Structure parameters

• Formula: C62 H68 B F24 P2 Rh
• Calculated formula: C62 H68 B F24 P2 Rh
• Title of publication: Solid‒State Molecular Organometallic Chemistry. Single‒Crystal to Single‒Crystal Reactivity and Catalysis with Light Hydrocarbon Substrates.
• Authors of publication: Chadwick, Fredrick M.; McKay, Alasdair I.; Martinez-Martinez, Antonio J.; Rees, Nick; Kraemer, Tobias; Macgregor, Stuart Alan; Weller, Andrew
• Journal of publication: Chem. Sci.
• Year of publication: 2017
• a: 19.2187 ± 0.0018 Å
• b: 17.1982 ± 0.0018 Å
• c: 19.999 ± 0.003 Å
• α: 90°
• β: 90.738 ± 0.012°
• γ: 90°
• Cell volume: 6609.7 ± 1.4 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.145
• Residual factor for significantly intense reflections: 0.1072
• Weighted residual factors for all reflections: 0.3333
• Weighted residual factors for significantly intense reflections: 0.2509
• Weighted residual factors for all reflections included in the refinement: 0.3327
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9981
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No