Information card for entry 1546623

Structure parameters

• Formula: C19 H28 O3 Si
• Calculated formula: C19 H28 O3 Si
• SMILES: [Si](Oc1c(c2c(cc1)[C@](C(=O)C=C2)(O)C)CC)(C(C)(C)C)(C)C
• Title of publication: Catalytic Asymmetric Hydroxylative Dearomatization of 2-Naphthols: Synthesis of Lacinilene Derivatives
• Authors of publication: Zhang, Yu; Liao, Yuting; Liu, Xiaohua; Xu, Xi; Lin, Lili; Feng, Xiaoming
• Journal of publication: Chem. Sci.
• Year of publication: 2017
• a: 21.9182 ± 0.0009 Å
• b: 6.1752 ± 0.0003 Å
• c: 14.8927 ± 0.0006 Å
• α: 90°
• β: 100.846 ± 0.004°
• γ: 90°
• Cell volume: 1979.71 ± 0.15 ų
• Cell temperature: 135 K
• Ambient diffraction temperature: 135 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0671
• Residual factor for significantly intense reflections: 0.0608
• Weighted residual factors for significantly intense reflections: 0.1649
• Weighted residual factors for all reflections included in the refinement: 0.1857
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No