Information card for entry 1546697

Structure parameters

• Chemical name: Hexaethylguanidinium tetrakis(trimethylsilylethynyl)borate diethyl ether monosolvate
• Formula: C37 H76 B N3 O Si4
• Calculated formula: C37 H76 B N3 O Si4
• Title of publication: Hexaethylguanidinium tetrakis(trimethylsilylethynyl)borate diethyl ether monosolvate
• Authors of publication: Oberparleiter, Stefan; Laus, Gerhard; Gelbrich, Thomas; Wurst, Klaus; Kunze-Liebhäuser, Julia; Schottenberger, Herwig
• Journal of publication: IUCrData
• Year of publication: 2017
• Journal volume: 2
• Journal issue: 5
• Pages of publication: x170724
• a: 12.9107 ± 0.0007 Å
• b: 17.872 ± 0.0008 Å
• c: 21.6094 ± 0.0011 Å
• α: 90°
• β: 95.0374 ± 0.0016°
• γ: 90°
• Cell volume: 4966.9 ± 0.4 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1089
• Residual factor for significantly intense reflections: 0.0679
• Weighted residual factors for significantly intense reflections: 0.1721
• Weighted residual factors for all reflections included in the refinement: 0.1931
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes