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Information card for entry 1547040
Preview
Coordinates | 1547040.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Ge-Sumanene |
---|---|
Chemical name | Ge-Sumanene |
Formula | C24 H24 Ge3 |
Calculated formula | C24 H24 Ge3 |
SMILES | [Ge]1(c2ccc3[Ge](c4c5c3c2c2c3c5c([Ge](c3ccc12)(C)C)cc4)(C)C)(C)C |
Title of publication | Synthesis of Silicon and Germanium-Containing Heterosumanenes via Rhodium-Catalyzed Cyclodehydrogenation of Silicon/Germanium-Hydrogen and Carbon-Hydrogen Bonds. |
Authors of publication | Zhou, Dandan; Gao, Ya; Liu, Bingxin; Tan, Qitao; Xu, Bin |
Journal of publication | Organic letters |
Year of publication | 2017 |
Journal volume | 19 |
Journal issue | 17 |
Pages of publication | 4628 - 4631 |
a | 12.121 ± 0.007 Å |
b | 20.805 ± 0.012 Å |
c | 19.049 ± 0.011 Å |
α | 90° |
β | 93.774 ± 0.008° |
γ | 90° |
Cell volume | 4793 ± 5 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 3 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1099 |
Residual factor for significantly intense reflections | 0.0494 |
Weighted residual factors for significantly intense reflections | 0.1091 |
Weighted residual factors for all reflections included in the refinement | 0.1355 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.939 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1547040.html
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