Information card for entry 1547540

Structure parameters

• Formula: C26.5 H31 Br2 Cl N2 Ni
• Calculated formula: C26.4999 H30.9998 Br2 Cl0.9998 N2 Ni
• Title of publication: Synthesis of hyperbranched low molecular weight polyethylene oils by an iminopyridine nickel(II) catalyst
• Authors of publication: D'Auria, Ilaria; Milione, Stefano; Caruso, Tonino; Balducci, Gabriele; Pellecchia, Claudio
• Journal of publication: Polym. Chem.
• Year of publication: 2017
• a: 14.21 ± 0.006 Å
• b: 14.561 ± 0.001 Å
• c: 14.996 ± 0.0017 Å
• α: 90°
• β: 110.079 ± 0.006°
• γ: 90°
• Cell volume: 2914.3 ± 1.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0442
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.1078
• Weighted residual factors for all reflections included in the refinement: 0.1127
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.7 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No