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Information card for entry 1548399
Preview
Coordinates | 1548399.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H29 Cl N2 O4 S |
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Calculated formula | C32 H29 Cl N2 O4 S |
Title of publication | Diastereo- and enantioselective [3 + 3] cycloaddition of spirocyclopropyl oxindoles using both aldonitrones and ketonitrones |
Authors of publication | Peng-Wei Xu; Jia-Kuan Liu; Lan Shen; Zhong-Yan Cao; Xiao-Li Zhao; Jun Yan; Jian Zhou |
Journal of publication | Nature Communications |
Year of publication | 2017 |
Journal volume | 8 |
Pages of publication | 1619 |
a | 8.9003 ± 0.0003 Å |
b | 13.1778 ± 0.0004 Å |
c | 13.2084 ± 0.0004 Å |
α | 108.296 ± 0.001° |
β | 102.628 ± 0.001° |
γ | 99.444 ± 0.001° |
Cell volume | 1389.26 ± 0.08 Å3 |
Ambient diffraction temperature | 160.01 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.057 |
Residual factor for significantly intense reflections | 0.0466 |
Weighted residual factors for significantly intense reflections | 0.0972 |
Weighted residual factors for all reflections included in the refinement | 0.1025 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.092 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1548399.html
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