Information card for entry 1548929

Structure parameters

• Formula: C49 H44 Br2 Cl2 F22 N2 Ni
• Calculated formula: C49 H44 Br2 Cl2 F22 N2 Ni
• Title of publication: Nickel and palladium complexes with fluorinated alkyl substituted α-diimine ligands for living/controlled olefin polymerization
• Authors of publication: Mundil, Robert; Sokolohorskyj, Anatolij; Hošek, Jan; Cvačka, Josef; Císařová, Ivana; Kvíčala, Jaroslav; Merna, Jan
• Journal of publication: Polymer Chemistry
• Year of publication: 2018
• Journal volume: 9
• Journal issue: 10
• Pages of publication: 1234
• a: 20.5269 ± 0.0014 Å
• b: 21.5497 ± 0.0014 Å
• c: 34.938 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 15455 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 72
• Hermann-Mauguin space group symbol: I b a m
• Hall space group symbol: -I 2 2c
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0591
• Weighted residual factors for significantly intense reflections: 0.167
• Weighted residual factors for all reflections included in the refinement: 0.1935
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No