Information card for entry 1549071

Structure parameters

• Formula: C75 H175 Ag19 Au O24 P12 S24
• Calculated formula: C75 H175 Ag18.9999 Au O24 P12 S24
• Title of publication: Synthesis, structural characterization and transformation of an eight-electron superatomic alloy, [Au@Ag₁₉{S₂P(OPr)₂}₁₂].
• Authors of publication: Lin, Yan-Ru; Kishore, Pilli V. V. N.; Liao, Jian-Hong; Kahlal, Samia; Liu, Yu-Chiao; Chiang, Ming-Hsi; Saillard, Jean-Yves; Liu, C. W.
• Journal of publication: Nanoscale
• Year of publication: 2018
• Journal volume: 10
• Journal issue: 15
• Pages of publication: 6855 - 6860
• a: 29.6903 ± 0.0007 Å
• b: 17.3784 ± 0.0004 Å
• c: 30.3868 ± 0.0006 Å
• α: 90°
• β: 110.373 ± 0.0006°
• γ: 90°
• Cell volume: 14697.9 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0574
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.1012
• Weighted residual factors for all reflections included in the refinement: 0.1153
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No