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Information card for entry 1549705
Preview
Coordinates | 1549705.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C52 H60 B F24 Fe P4 |
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Calculated formula | C52 H60 B F24 Fe P4 |
Title of publication | Reversible coordination of N<sub>2</sub> and H<sub>2</sub> to a homoleptic <i>S</i> = 1/2 Fe(i) diphosphine complex in solution and the solid state. |
Authors of publication | Doyle, Laurence R.; Scott, Daniel J.; Hill, Peter J.; Fraser, Duncan A. X.; Myers, William K.; White, Andrew J. P.; Green, Jennifer C.; Ashley, Andrew E. |
Journal of publication | Chemical science |
Year of publication | 2018 |
Journal volume | 9 |
Journal issue | 37 |
Pages of publication | 7362 - 7369 |
a | 13.2989 ± 0.0003 Å |
b | 13.2989 ± 0.0003 Å |
c | 17.4417 ± 0.0006 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3084.75 ± 0.14 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 82 |
Hermann-Mauguin space group symbol | I -4 |
Hall space group symbol | I -4 |
Residual factor for all reflections | 0.0596 |
Residual factor for significantly intense reflections | 0.0466 |
Weighted residual factors for significantly intense reflections | 0.0997 |
Weighted residual factors for all reflections included in the refinement | 0.1067 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1549705.html
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