Crystallography Open Database

Information card for entry 1549723

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Coordinates	1549723.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H19 Cl4 Rh
Calculated formula	C24 H19 Cl4 Rh
Title of publication	Divergent ring-opening coupling between cyclopropanols and alkynes under cobalt catalysis.
Authors of publication	Yang, Junfeng; Shen, Yixiao; Lim, Yang Jie; Yoshikai, Naohiko
Journal of publication	Chemical science
Year of publication	2018
Journal volume	9
Journal issue	34
Pages of publication	6928 - 6934
a	14.3151 ± 0.0003 Å
b	6.8774 ± 0.0001 Å
c	23.4347 ± 0.0005 Å
α	90°
β	106.959 ± 0.0007°
γ	90°
Cell volume	2206.84 ± 0.07 Å³
Cell temperature	190 ± 2 K
Ambient diffraction temperature	190 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0387
Residual factor for significantly intense reflections	0.0292
Weighted residual factors for significantly intense reflections	0.0611
Weighted residual factors for all reflections included in the refinement	0.066
Goodness-of-fit parameter for all reflections included in the refinement	1.043
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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