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Information card for entry 1550231
Preview
Coordinates | 1550231.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C102 H146 In2 K2 N6 O2 Si4 |
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Calculated formula | C102 H146 In2 K2 N6 O2 Si4 |
SMILES | [In]1(N([Si](O[Si](N1c1c(C(C)C)cccc1C(C)C)(C)C)(C)C)c1c(cccc1C(C)C)C(C)C)N([K])c1c(cc(cc1C)C)C.c1(ccccc1)C.c1(ccccc1)C |
Title of publication | Reduction of Organic Azides by Indyl-Anions. Isolation and Reactivity Studies of Indium-Nitrogen Multiple Bonds |
Authors of publication | Anker, Mathew; Lein, Matthias; Coles, Martyn P. |
Journal of publication | Chemical Science |
Year of publication | 2019 |
a | 23.6145 ± 0.0004 Å |
b | 17.0543 ± 0.0003 Å |
c | 25.7456 ± 0.0004 Å |
α | 90° |
β | 97.4553 ± 0.0014° |
γ | 90° |
Cell volume | 10280.8 ± 0.3 Å3 |
Cell temperature | 119.99 ± 0.1 K |
Ambient diffraction temperature | 119.99 ± 0.1 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0511 |
Residual factor for significantly intense reflections | 0.0374 |
Weighted residual factors for significantly intense reflections | 0.0877 |
Weighted residual factors for all reflections included in the refinement | 0.095 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.009 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1550231.html
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