Information card for entry 1550732

Structure parameters

• Formula: C25 H44 K N2 O6 Rh0.33 Sn4
• Calculated formula: C25 H44 K N2 O6 Rh0.333333 Sn4
• Title of publication: Synthesis and Structure of a Family of Rhodium Polystannide Clusters [Rh@Sn10]3‒, [Rh@Sn12]3‒, [Rh2@Sn17]6‒ and the First Triply-Fused Stannide, [Rh3@Sn24]5‒
• Authors of publication: Liu, Chao; Jin, Xiao; Li, Leijiao; Xu, Jun; McGrady, John E.; Sun, Zhong-Ming
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 24.749 ± 0.003 Å
• b: 24.749 Å
• c: 29.868 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 15844 ± 2 ų
• Cell temperature: 120.15 K
• Ambient diffraction temperature: 120.15 K
• Number of distinct elements: 7
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0638
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for significantly intense reflections: 0.0875
• Weighted residual factors for all reflections included in the refinement: 0.0973
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No