Information card for entry 1550734

Structure parameters

• Formula: C62 H140 K6 N14 O18 Rh2 Sn17
• Calculated formula: C62.5 H138 K6 N13.5 O18 Rh2 Sn17
• Title of publication: Synthesis and Structure of a Family of Rhodium Polystannide Clusters [Rh@Sn10]3‒, [Rh@Sn12]3‒, [Rh2@Sn17]6‒ and the First Triply-Fused Stannide, [Rh3@Sn24]5‒
• Authors of publication: Liu, Chao; Jin, Xiao; Li, Leijiao; Xu, Jun; McGrady, John E.; Sun, Zhong-Ming
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 21.5558 ± 0.0014 Å
• b: 16.1668 ± 0.001 Å
• c: 33.205 ± 0.002 Å
• α: 90°
• β: 97.828 ± 0.001°
• γ: 90°
• Cell volume: 11463.7 ± 1.2 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0387
• Residual factor for significantly intense reflections: 0.0292
• Weighted residual factors for significantly intense reflections: 0.0604
• Weighted residual factors for all reflections included in the refinement: 0.0643
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No