Information card for entry 1551622

Structure parameters

• Formula: C30 H52 N2 O10 V2
• Calculated formula: C30 H52 N2 O10 V2
• Title of publication: Synthesis and Crystal Structures of Dinuclear Dioxidovanadium(V) and Tetranuclear Oxidovanadium(IV) Complexes with 2,6-Bis(hydroxymethyl)-4-methylphenol
• Authors of publication: MIKURIYA, Masahiro; FUKUTANI, Masami; YOSHIOKA, Daisuke
• Journal of publication: X-ray Structure Analysis Online
• Year of publication: 2015
• Journal volume: 31
• Journal issue: 0
• Pages of publication: 33
• a: 8.5059 ± 0.0015 Å
• b: 9.8815 ± 0.0017 Å
• c: 11.3339 ± 0.0019 Å
• α: 82.916 ± 0.003°
• β: 83.819 ± 0.003°
• γ: 65.595 ± 0.003°
• Cell volume: 859.2 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0594
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for significantly intense reflections: 0.1022
• Weighted residual factors for all reflections included in the refinement: 0.1166
• Goodness-of-fit parameter for all reflections included in the refinement: 0.93
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No