Information card for entry 1551700

Structure parameters

• Formula: C32 H45 B N6 Ru
• Calculated formula: C32 H45 B N6 Ru
• Title of publication: Crystal Structure of (Cycloocta-1,5-diene)tris(hydrazine)hydrido-ruthenium(II) tetraphenylborate
• Authors of publication: OWALUDE, Samson O.; EKE, Uche B.; ODEBUNMI, Ezekiel O.; NESTEROV, Vladimir N.; MEIJBOOM, Reinout; COVILLE, Neil J.
• Journal of publication: X-ray Structure Analysis Online
• Year of publication: 2012
• Journal volume: 28
• Pages of publication: 29
• a: 9.7449 ± 0.0008 Å
• b: 32.881 ± 0.003 Å
• c: 18.6962 ± 0.0016 Å
• α: 90°
• β: 99.571 ± 0.001°
• γ: 90°
• Cell volume: 5907.3 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0499
• Residual factor for significantly intense reflections: 0.0392
• Weighted residual factors for significantly intense reflections: 0.0909
• Weighted residual factors for all reflections included in the refinement: 0.0984
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No