Crystallography Open Database

Information card for entry 1551989

1551988 << 1551989 >> 1551990

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Coordinates	1551989.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H73 Cr2 N4
Calculated formula	C65 H73 Cr2 N4
Title of publication	Carboalumination of a chromium-chromium quintuple bond
Authors of publication	Awal Noor; Germund Glatz; Robert Muller; Martin Kaupp; Serhiy Demeshko; Rhett Kempe
Journal of publication	Nature Chemistry
Year of publication	2009
Journal volume	1
Pages of publication	322 - 325
a	11.993 ± 0.0009 Å
b	12.5339 ± 0.001 Å
c	12.5675 ± 0.001 Å
α	62.264 ± 0.006°
β	77.005 ± 0.006°
γ	63.04 ± 0.006°
Cell volume	1490.1 ± 0.2 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0814
Residual factor for significantly intense reflections	0.064
Weighted residual factors for significantly intense reflections	0.186
Weighted residual factors for all reflections included in the refinement	0.1947
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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