Crystallography Open Database

Information card for entry 1552002

1552001 << 1552002 >> 1552003

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Coordinates	1552002.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H56 B Cl Ge N4
Calculated formula	C37 H56 B Cl Ge N4
SMILES	[Ge](Cl)(B1N(C=CN1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C)=C1N(C(C)C)C(C)=C(N1C(C)C)C
Title of publication	A stable heavier group 14 analogue of vinylidene
Authors of publication	Arnab Rit; Jesus Campos; Haoyu Niu; Simon Aldridge
Journal of publication	Nature Chemistry
Year of publication	2016
Journal volume	8
Pages of publication	1022 - 1026
a	31.5447 ± 0.0004 Å
b	15.1571 ± 0.0002 Å
c	16.326 ± 0.0003 Å
α	90°
β	102.94 ± 0.0007°
γ	90°
Cell volume	7607.7 ± 0.2 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0631
Residual factor for significantly intense reflections	0.0469
Weighted residual factors for all reflections	0.1164
Weighted residual factors for significantly intense reflections	0.1011
Weighted residual factors for all reflections included in the refinement	0.1164
Goodness-of-fit parameter for all reflections included in the refinement	0.9075
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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