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Information card for entry 1552033
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Coordinates | 1552033.cif |
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Original paper (by DOI) | HTML |
Formula | C39.55 H40.72 Cl7 P Rh2 Si2 |
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Calculated formula | C39.549 H40.728 Cl7 P Rh2 Si2 |
Title of publication | Low-valent Homobimetallic Rh Complexes: Influence of Ligands on the Structure and the Intramolecular Reactivity of Rh‒H Intermediates |
Authors of publication | Jurt, Pascal; Salnikov, Oleg; Gianetti, Thomas L.; Chukanov, Nikita; Baker, Matthew G.; Le Corre, Grégoire; Borger, Jaap E.; Verel, René; Gauthier, Sébastien; Fuhr, Olaf; Kovtunov, Kirill V.; Fedorov, Alexey; Fenske, Dieter; Koptyug, Igor V.; Grützmacher, Hansjörg |
Journal of publication | Chemical Science |
Year of publication | 2019 |
a | 14.3566 ± 0.0004 Å |
b | 13.3287 ± 0.0003 Å |
c | 23.2251 ± 0.0007 Å |
α | 90° |
β | 99.837 ± 0.002° |
γ | 90° |
Cell volume | 4378.9 ± 0.2 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0511 |
Residual factor for significantly intense reflections | 0.0429 |
Weighted residual factors for significantly intense reflections | 0.0725 |
Weighted residual factors for all reflections included in the refinement | 0.0746 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.235 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/1552033.html
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