Information card for entry 1552185

Structure parameters

• Formula: C54 H92 O20 P4 Sn6
• Calculated formula: C54 H92 O20 P4 Sn6
• Title of publication: Assembly of High-Nuclearity Sn26, Sn34-Oxo Clusters: Solvent Strategy and Inorganic Sn Incorporation
• Authors of publication: Zhu, Yu; Zhang, Lei; Zhang, Jian
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 26.5875 ± 0.0005 Å
• b: 12.3043 ± 0.0002 Å
• c: 22.3663 ± 0.0004 Å
• α: 90°
• β: 98.407 ± 0.002°
• γ: 90°
• Cell volume: 7238.3 ± 0.2 ų
• Cell temperature: 296.76 ± 0.1 K
• Ambient diffraction temperature: 296.76 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0443
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.1046
• Weighted residual factors for all reflections included in the refinement: 0.1098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No