Crystallography Open Database

Information card for entry 1552187

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Coordinates	1552187.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C114 H272 Cl4 N32 O74 Sn26
Calculated formula	C106.528 H216 Cl4 N24 O60 Sn26
Title of publication	Assembly of High-Nuclearity Sn26, Sn34-Oxo Clusters: Solvent Strategy and Inorganic Sn Incorporation
Authors of publication	Zhu, Yu; Zhang, Lei; Zhang, Jian
Journal of publication	Chemical Science
Year of publication	2019
a	16.154 ± 0.013 Å
b	18.36 ± 0.016 Å
c	23.56 ± 0.02 Å
α	73.021 ± 0.008°
β	89.189 ± 0.01°
γ	68.918 ± 0.011°
Cell volume	6203 ± 9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1443
Residual factor for significantly intense reflections	0.0873
Weighted residual factors for significantly intense reflections	0.1262
Weighted residual factors for all reflections included in the refinement	0.1425
Goodness-of-fit parameter for all reflections included in the refinement	1.137
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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