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Information card for entry 1552972
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Coordinates | 1552972.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C17 H21 B Br O P |
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Calculated formula | C17 H21 B Br O P |
Title of publication | Palladium-catalyzed 1,4-addition of secondary alkylphenylphosphines to α,β-unsaturated carbonyl compounds for the synthesis of phosphorus- and carbon-stereogenic compounds |
Authors of publication | Li, Chun; Bian, Qing-Long; Xu, Sheng; Duan, Wei-Liang |
Journal of publication | Org. Chem. Front. |
Year of publication | 2014 |
Journal volume | 1 |
Journal issue | 5 |
Pages of publication | 541 |
a | 6.4951 ± 0.0015 Å |
b | 9.549 ± 0.002 Å |
c | 15.501 ± 0.004 Å |
α | 81.333 ± 0.005° |
β | 86.707 ± 0.005° |
γ | 74.351 ± 0.005° |
Cell volume | 915 ± 0.4 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 1 |
Hermann-Mauguin space group symbol | P 1 |
Hall space group symbol | P 1 |
Residual factor for all reflections | 0.0789 |
Residual factor for significantly intense reflections | 0.0552 |
Weighted residual factors for significantly intense reflections | 0.1448 |
Weighted residual factors for all reflections included in the refinement | 0.1598 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1552972.html
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