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Information card for entry 1552974
Preview
Coordinates | 1552974.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H28 B O P |
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Calculated formula | C24 H28 B O P |
SMILES | [P@]([BH3])([C@@H](CC(=O)c1ccccc1)c1ccccc1)(C(C)C)c1ccccc1 |
Title of publication | Palladium-catalyzed 1,4-addition of secondary alkylphenylphosphines to α,β-unsaturated carbonyl compounds for the synthesis of phosphorus- and carbon-stereogenic compounds |
Authors of publication | Li, Chun; Bian, Qing-Long; Xu, Sheng; Duan, Wei-Liang |
Journal of publication | Org. Chem. Front. |
Year of publication | 2014 |
Journal volume | 1 |
Journal issue | 5 |
Pages of publication | 541 |
a | 10.135 ± 0.007 Å |
b | 13.483 ± 0.009 Å |
c | 15.598 ± 0.01 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2131 ± 2 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0383 |
Residual factor for significantly intense reflections | 0.0355 |
Weighted residual factors for significantly intense reflections | 0.0902 |
Weighted residual factors for all reflections included in the refinement | 0.0924 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1552974.html
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