Information card for entry 1553131

Structure parameters

• Chemical name: (POX)PdCl2
• Formula: C16 H24 Cl2 N2 O Pd
• Calculated formula: C16 H24 Cl2 N2 O Pd
• Title of publication: Pd(ii)-catalyzed intermolecular enantioselective hydroamination of styrenes
• Authors of publication: Yu, Feng; Chen, Pinhong; Liu, Guosheng
• Journal of publication: Organic Chemistry Frontiers
• Year of publication: 2015
• Journal volume: 2
• Journal issue: 7
• Pages of publication: 819
• a: 12.1876 ± 0.0018 Å
• b: 9.8204 ± 0.0014 Å
• c: 15.854 ± 0.002 Å
• α: 90°
• β: 96.796 ± 0.003°
• γ: 90°
• Cell volume: 1884.2 ± 0.5 ų
• Cell temperature: 130 K
• Ambient diffraction temperature: 130 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0974
• Residual factor for significantly intense reflections: 0.0638
• Weighted residual factors for significantly intense reflections: 0.118
• Weighted residual factors for all reflections included in the refinement: 0.1327
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No