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Information card for entry 1554281
Preview
Coordinates | 1554281.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C9 H6 N O |
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Calculated formula | C9 H6 N O |
Title of publication | Photo-induced C‒H bond activation of N,N′-dialkylethylenediamine upon aza-Michael addition to 1,8-pyrenedione: facile synthesis of fluorescent pyrene derivatives |
Authors of publication | Yao, Wei; Sun, Mingtai; Zhang, Yuannian; Yang, Hui; Liang, Dong; Wu, Haixia; Ni, Runyan; Wong, Ming Wah; Huang, Dejian |
Journal of publication | Organic Chemistry Frontiers |
Year of publication | 2018 |
Journal volume | 5 |
Journal issue | 10 |
Pages of publication | 1679 |
a | 13.3145 ± 0.0004 Å |
b | 13.4792 ± 0.0004 Å |
c | 7.0709 ± 0.0002 Å |
α | 90° |
β | 93.942 ± 0.001° |
γ | 90° |
Cell volume | 1266 ± 0.06 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0413 |
Residual factor for significantly intense reflections | 0.0383 |
Weighted residual factors for significantly intense reflections | 0.1095 |
Weighted residual factors for all reflections included in the refinement | 0.1143 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.092 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1554281.html
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Users of the data should acknowledge the original authors of the
structural data.