Crystallography Open Database

Information card for entry 1554733

Preview

Coordinates	1554733.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H19 Cl O
Calculated formula	C26 H19 Cl O
Title of publication	Convenient construction of dibenzo[b,d]furanes and 2,6-diaryl-4-(2-hydroxyphenyl)pyridines via domino reaction of pyridinium ylides with 2-aryl-3-nitrochromenes
Authors of publication	Sun, Jing; Jiang, Wang; Yan, Chao-Guo
Journal of publication	Organic Chemistry Frontiers
Year of publication	2019
Journal volume	6
Journal issue	9
Pages of publication	1428
a	9.998 ± 0.007 Å
b	15.063 ± 0.011 Å
c	15.716 ± 0.011 Å
α	63.252 ± 0.013°
β	83.527 ± 0.015°
γ	76.536 ± 0.016°
Cell volume	2055 ± 3 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.4157
Residual factor for significantly intense reflections	0.1326
Weighted residual factors for significantly intense reflections	0.2689
Weighted residual factors for all reflections included in the refinement	0.3894
Goodness-of-fit parameter for all reflections included in the refinement	1.006
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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