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Information card for entry 1554808
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Coordinates | 1554808.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | 6a in manuscript |
---|---|
Formula | C27 H23 N O |
Calculated formula | C27 H23 N O |
Title of publication | Direct access to benzo[b]fluorenes via a gold-catalysed A3-coupling strategy |
Authors of publication | Lustosa, Danilo M.; Cieslik, Patrick; Hartmann, Deborah; Bruckhoff, Tim; Rudolph, Matthias; Rominger, Frank; Hashmi, A. Stephen K. |
Journal of publication | Organic Chemistry Frontiers |
Year of publication | 2019 |
Journal volume | 6 |
Journal issue | 10 |
Pages of publication | 1655 |
a | 6.7344 ± 0.0004 Å |
b | 18.9552 ± 0.0012 Å |
c | 15.1244 ± 0.0008 Å |
α | 90° |
β | 90.856 ± 0.004° |
γ | 90° |
Cell volume | 1930.4 ± 0.2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.1004 |
Residual factor for significantly intense reflections | 0.0799 |
Weighted residual factors for significantly intense reflections | 0.2324 |
Weighted residual factors for all reflections included in the refinement | 0.2432 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.578 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1554808.html
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