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Information card for entry 1554937
Preview
Coordinates | 1554937.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C133 H116 N8 O21 S4 |
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Calculated formula | C133 H112 N8 O21 S4 |
Title of publication | Rapid access to spirocylic oxindoles: application of asymmetric N-heterocyclic carbene-catalyzed [3 + 3] cycloaddition of imines to oxindole-derived enals. |
Authors of publication | Xie, Danbo; Yang, Limin; Lin, Youqiang; Zhang, Zhiming; Chen, Dongdong; Zeng, Xiaofei; Zhong, Guofu |
Journal of publication | Organic letters |
Year of publication | 2015 |
Journal volume | 17 |
Journal issue | 10 |
Pages of publication | 2318 - 2321 |
a | 10.8299 ± 0.0004 Å |
b | 17.8426 ± 0.0007 Å |
c | 16.7462 ± 0.0006 Å |
α | 90° |
β | 105.418 ± 0.004° |
γ | 90° |
Cell volume | 3119.5 ± 0.2 Å3 |
Cell temperature | 223 ± 2 K |
Ambient diffraction temperature | 223 ± 2 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0898 |
Residual factor for significantly intense reflections | 0.071 |
Weighted residual factors for significantly intense reflections | 0.1937 |
Weighted residual factors for all reflections included in the refinement | 0.2096 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.057 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1554937.html
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