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Information card for entry 1555236
Preview
Coordinates | 1555236.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C14 H17 F O2 |
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Calculated formula | C14 H17 F O2 |
SMILES | F[C@H]1[C@H]([C@H]1c1ccccc1)[C@@H]1OC(OC1)(C)C |
Title of publication | Diastereoselective Fluorocyclopropanation of Chiral Allylic Alcohols Using an α-Fluoroiodomethylzinc Carbenoid. |
Authors of publication | Navuluri, Chandrasekhar; Charette, André B |
Journal of publication | Organic letters |
Year of publication | 2015 |
Journal volume | 17 |
Journal issue | 17 |
Pages of publication | 4288 - 4291 |
a | 5.8616 ± 0.0002 Å |
b | 11.0435 ± 0.0004 Å |
c | 18.6965 ± 0.0008 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1210.27 ± 0.08 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0251 |
Residual factor for significantly intense reflections | 0.0241 |
Weighted residual factors for significantly intense reflections | 0.0579 |
Weighted residual factors for all reflections included in the refinement | 0.0586 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.048 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.34139 Å |
Diffraction radiation type | GaKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1555236.html
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