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Information card for entry 1555524
Preview
Coordinates | 1555524.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C20 H14 |
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Calculated formula | C20 H14 |
SMILES | c1(cc2ccccc2cc1)/C=C(\C#C)c1ccccc1 |
Title of publication | Cu(I)-Catalyzed Tandem Reaction of Carbene Coupling and Horner-Wadsworth-Emmons Type Olefination: Access toward Enynes. |
Authors of publication | Zhou, Yujing; Ye, Fei; Zhou, Qi; Zhang, Yan; Wang, Jianbo |
Journal of publication | Organic letters |
Year of publication | 2016 |
Journal volume | 18 |
Journal issue | 9 |
Pages of publication | 2024 - 2027 |
a | 6.4855 ± 0.0007 Å |
b | 7.5481 ± 0.0006 Å |
c | 13.9074 ± 0.0011 Å |
α | 90° |
β | 95.824 ± 0.009° |
γ | 90° |
Cell volume | 677.3 ± 0.11 Å3 |
Cell temperature | 180 ± 0.1 K |
Ambient diffraction temperature | 180 ± 0.1 K |
Number of distinct elements | 2 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0645 |
Residual factor for significantly intense reflections | 0.0466 |
Weighted residual factors for significantly intense reflections | 0.0963 |
Weighted residual factors for all reflections included in the refinement | 0.1096 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.13 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1555524.html
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