Information card for entry 1555649

Structure parameters

• Formula: C16 H19 B N2 O3
• Calculated formula: C16 H19 B N2 O3
• Title of publication: Rhodium-Catalyzed C6-Selective C-H Borylation of 2-Pyridones.
• Authors of publication: Miura, Wataru; Hirano, Koji; Miura, Masahiro
• Journal of publication: Organic letters
• Year of publication: 2016
• Journal volume: 18
• Journal issue: 15
• Pages of publication: 3742 - 3745
• a: 10.4857 ± 0.0015 Å
• b: 10.8482 ± 0.001 Å
• c: 14.0338 ± 0.0011 Å
• α: 70.4935 ± 0.001°
• β: 89.135 ± 0.016°
• γ: 89.14 ± 0.02°
• Cell volume: 1504.5 ± 0.3 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0581
• Weighted residual factors for all reflections included in the refinement: 0.1459
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No