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Information card for entry 1555736
Preview
Coordinates | 1555736.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C51 H18 F51 I3 N6 O3 |
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Calculated formula | C51 H18 F51 I3 N6 O3 |
Title of publication | Halogen-Bond-Promoted Double Radical Isocyanide Insertion under Visible-Light Irradiation: Synthesis of 2-Fluoroalkylated Quinoxalines. |
Authors of publication | Sun, Xiaoyang; Wang, Wenmin; Li, Yanle; Ma, Jing; Yu, Shouyun |
Journal of publication | Organic letters |
Year of publication | 2016 |
Journal volume | 18 |
Journal issue | 18 |
Pages of publication | 4638 - 4641 |
a | 11.539 ± 0.0013 Å |
b | 16.419 ± 0.002 Å |
c | 18.984 ± 0.002 Å |
α | 77.096 ± 0.002° |
β | 85.285 ± 0.002° |
γ | 73.926 ± 0.002° |
Cell volume | 3368 ± 0.7 Å3 |
Cell temperature | 300 K |
Ambient diffraction temperature | 300 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.116 |
Residual factor for significantly intense reflections | 0.0639 |
Weighted residual factors for significantly intense reflections | 0.17 |
Weighted residual factors for all reflections included in the refinement | 0.2052 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.017 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1555736.html
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Users of the data should acknowledge the original authors of the
structural data.