Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 1555750
Preview
Coordinates | 1555750.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H49 Li Ni O8 |
---|---|
Calculated formula | C30 H49 Li Ni O8 |
Title of publication | Multicomponent Coupling Reaction of Perfluoroarenes with 1,3-Butadiene and Aryl Grignard Reagents Promoted by an Anionic Ni(II) Complex. |
Authors of publication | Iwasaki, Takanori; Fukuoka, Asuka; Min, Xin; Yokoyama, Wataru; Kuniyasu, Hitoshi; Kambe, Nobuaki |
Journal of publication | Organic letters |
Year of publication | 2016 |
Journal volume | 18 |
Journal issue | 19 |
Pages of publication | 4868 - 4871 |
a | 8.67174 ± 0.00016 Å |
b | 12.0843 ± 0.0002 Å |
c | 15.4857 ± 0.0003 Å |
α | 86.329 ± 0.0008° |
β | 78.921 ± 0.0008° |
γ | 74.044 ± 0.0008° |
Cell volume | 1531.07 ± 0.05 Å3 |
Cell temperature | 123 K |
Ambient diffraction temperature | 123 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0465 |
Residual factor for significantly intense reflections | 0.0415 |
Weighted residual factors for significantly intense reflections | 0.1162 |
Weighted residual factors for all reflections included in the refinement | 0.1193 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.075 |
Diffraction radiation wavelength | 1.54187 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1555750.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.