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Information card for entry 1555819
Preview
Coordinates | 1555819.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H25 O2 P Se |
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Calculated formula | C30 H25 O2 P Se |
SMILES | [Se]=P1(Oc2c(c3ccccc3cc2)c2c(O1)ccc1ccccc21)[C@@H](C)[C@H](C)c1ccccc1 |
Title of publication | Sequential Deprotonation-Alkylation of Binaphthyloxy-Substituted Phosphonochalcogenoates: Chiral Tri- and Tetrasubstituted Carbon Centers Adjacent to a Phosphorus Atom. |
Authors of publication | Maekawa, Yuuki; Maruyama, Toshifumi; Murai, Toshiaki |
Journal of publication | Organic letters |
Year of publication | 2016 |
Journal volume | 18 |
Journal issue | 20 |
Pages of publication | 5264 - 5267 |
a | 7.48 ± 0.002 Å |
b | 16.779 ± 0.004 Å |
c | 19.319 ± 0.005 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2424.7 ± 1.1 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.1112 |
Residual factor for significantly intense reflections | 0.0665 |
Weighted residual factors for significantly intense reflections | 0.1068 |
Weighted residual factors for all reflections included in the refinement | 0.1273 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1555819.html
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