Information card for entry 1555824

Structure parameters

• Formula: C27 H28 O9 S
• Calculated formula: C27 H28 O9 S
• Title of publication: Stereoselective Radical Cyclization Cascades Triggered by Addition of Diverse Radicals to Alkynes To Construct 6(5)-6-5 Fused Rings.
• Authors of publication: Huang, Lin; Ye, Liu; Li, Xiao-Hua; Li, Zhong-Liang; Lin, Jin-Shun; Liu, Xin-Yuan
• Journal of publication: Organic letters
• Year of publication: 2016
• Journal volume: 18
• Journal issue: 20
• Pages of publication: 5284 - 5287
• a: 9.7672 ± 0.0004 Å
• b: 11.7742 ± 0.0004 Å
• c: 24.7073 ± 0.0009 Å
• α: 101.224 ± 0.001°
• β: 93.188 ± 0.001°
• γ: 112.05 ± 0.001°
• Cell volume: 2557.16 ± 0.17 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0344
• Residual factor for significantly intense reflections: 0.0341
• Weighted residual factors for significantly intense reflections: 0.0858
• Weighted residual factors for all reflections included in the refinement: 0.0861
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No