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Information card for entry 1555904
Preview
Coordinates | 1555904.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H19 N O5 |
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Calculated formula | C21 H19 N O5 |
SMILES | N(=O)(=O)c1ccc(cc1)/C=C/CC1(Cc2ccccc2C1=O)C(=O)OCC |
Title of publication | Relay Rh(II)/Pd(0) Dual Catalysis: Selective Construction of Cyclic All-Quaternary Carbon Centers. |
Authors of publication | Chen, Zi-Sheng; Huang, Xiao-Yan; Gao, Jin-Ming; Ji, Kegong |
Journal of publication | Organic letters |
Year of publication | 2016 |
Journal volume | 18 |
Journal issue | 22 |
Pages of publication | 5876 - 5879 |
a | 24.915 ± 0.013 Å |
b | 10.604 ± 0.005 Å |
c | 15.39 ± 0.008 Å |
α | 90° |
β | 113.315 ± 0.009° |
γ | 90° |
Cell volume | 3734 ± 3 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.1859 |
Residual factor for significantly intense reflections | 0.1141 |
Weighted residual factors for significantly intense reflections | 0.3437 |
Weighted residual factors for all reflections included in the refinement | 0.3997 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.245 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1555904.html
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Users of the data should acknowledge the original authors of the
structural data.