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Information card for entry 1556074
Preview
Coordinates | 1556074.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C16 H18.18 N2.18 O2.55 S0.73 |
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Calculated formula | C16 H18.1818 N2.18182 O2.54545 S0.727273 |
Title of publication | Catalyst-Free "On-Water" Regio- and Stereospecific Ring-Opening of Spiroaziridine Oxindole: Enantiopure Synthesis of Unsymmetrical 3,3'-Bisindoles. |
Authors of publication | Hajra, Saumen; Singha Roy, Somnath; Aziz, Sk Mohammad; Das, Dhiraj |
Journal of publication | Organic letters |
Year of publication | 2017 |
Journal volume | 19 |
Journal issue | 15 |
Pages of publication | 4082 - 4085 |
a | 12.3073 ± 0.0015 Å |
b | 18.643 ± 0.002 Å |
c | 20.256 ± 0.002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 4647.6 ± 0.9 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.1335 |
Residual factor for significantly intense reflections | 0.0704 |
Weighted residual factors for significantly intense reflections | 0.1726 |
Weighted residual factors for all reflections included in the refinement | 0.201 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.978 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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