Information card for entry 1556284

Structure parameters

• Formula: C16 H24 Cl2 N2 O4 Pd S2
• Calculated formula: C16 H24 Cl2 N2 O4 Pd S2
• Title of publication: Conjugate addition of arylboronic acids to α,β-unsaturated carbonyl compounds in aqueous medium using Pd(ii) complexes with dihydroxy-2,2′-bipyridine ligands: homogeneous or heterogeneous nano-catalysis?
• Authors of publication: Tomás-Mendivil, Eder; Díez, Josefina; Cadierno, Victorio
• Journal of publication: Catalysis Science & Technology
• Year of publication: 2011
• Journal volume: 1
• Journal issue: 9
• Pages of publication: 1605
• a: 8.4783 ± 0.0003 Å
• b: 11.6061 ± 0.0004 Å
• c: 13.1535 ± 0.0005 Å
• α: 67.125 ± 0.004°
• β: 89.797 ± 0.003°
• γ: 68.971 ± 0.004°
• Cell volume: 1099.1 ± 0.09 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0335
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for significantly intense reflections: 0.0816
• Weighted residual factors for all reflections included in the refinement: 0.0839
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No