Information card for entry 1556353

Structure parameters

• Formula: C65 H53 K3 N9 O4 Tb
• Calculated formula: C65 H53 K3 N9 O4 Tb
• Title of publication: Multielectron redox chemistry of lanthanide Schiff-base complexes
• Authors of publication: Camp, Clément; Guidal, Valentin; Biswas, Biplab; Pécaut, Jacques; Dubois, Lionel; Mazzanti, Marinella
• Journal of publication: Chemical Science
• Year of publication: 2012
• Journal volume: 3
• Journal issue: 8
• Pages of publication: 2433
• a: 14.5693 ± 0.0013 Å
• b: 30.262 ± 0.003 Å
• c: 14.6011 ± 0.0013 Å
• α: 90°
• β: 108.494 ± 0.009°
• γ: 90°
• Cell volume: 6105.1 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1479
• Residual factor for significantly intense reflections: 0.1004
• Weighted residual factors for significantly intense reflections: 0.2392
• Weighted residual factors for all reflections included in the refinement: 0.2722
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No