Information card for entry 1556356

Structure parameters

• Formula: C65 H112 Ni2 P10
• Calculated formula: C65 H112 Ni2 P10
• Title of publication: Bicyclic dinuclear tris-(ditopic diphosphane) complexes of zerovalent group 10 metals
• Authors of publication: Tofan, Daniel; Cummins, Christopher C.
• Journal of publication: Chemical Science
• Year of publication: 2012
• Journal volume: 3
• Journal issue: 8
• Pages of publication: 2474
• a: 11.3941 ± 0.0002 Å
• b: 12.6121 ± 0.0002 Å
• c: 14.341 ± 0.0002 Å
• α: 66.008 ± 0.001°
• β: 82.323 ± 0.001°
• γ: 66.713 ± 0.001°
• Cell volume: 1728.51 ± 0.05 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0458
• Residual factor for significantly intense reflections: 0.0408
• Weighted residual factors for significantly intense reflections: 0.1111
• Weighted residual factors for all reflections included in the refinement: 0.1159
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No