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Information card for entry 1556373
Preview
Coordinates | 1556373.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C19 H24 Br2 Cl2 N4 Ni |
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Calculated formula | C19 H24 Br2 Cl2 N4 Ni |
Title of publication | Tandem ethylene oligomerisation and Friedel‒Crafts alkylation of toluene catalysed by bis-(3,5-dimethylpyrazol-1-ylmethyl)benzene nickel(ii) complexes and ethylaluminium dichloride |
Authors of publication | Budhai, Asheena; Omondi, Bernard; Ojwach, Stephen O.; Obuah, Collins; Osei-Twum, Emmanuel Y.; Darkwa, James |
Journal of publication | Catalysis Science & Technology |
Year of publication | 2013 |
Journal volume | 3 |
Journal issue | 12 |
Pages of publication | 3130 |
a | 14.2034 ± 0.0007 Å |
b | 11.5066 ± 0.0007 Å |
c | 14.6836 ± 0.0011 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2399.8 ± 0.3 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 20 |
Hermann-Mauguin space group symbol | C 2 2 21 |
Hall space group symbol | C 2c 2 |
Residual factor for all reflections | 0.0473 |
Residual factor for significantly intense reflections | 0.0445 |
Weighted residual factors for significantly intense reflections | 0.1204 |
Weighted residual factors for all reflections included in the refinement | 0.1225 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.06 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1556373.html
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