Information card for entry 1556431

Structure parameters

• Formula: C354.9 H199.8 Al6 Cl1.8 N24 O18
• Calculated formula: C354.9 H199.8 Al6 Cl1.8 N24 O18
• Title of publication: Propeller-Shaped Aluminum Complexes with an Azaperylene Core in the Ligands
• Authors of publication: Tsukao, M.; Hashikawa, Y.; Toyama, N.; Muraoka, M.; Murata, M.; Sasamori, T.; Wakamiya, A.; Murata, Y.
• Journal of publication: Inorganics
• Year of publication: 2019
• Journal volume: 7
• Pages of publication: 109
• a: 34.0652 ± 0.0003 Å
• b: 34.0652 ± 0.0003 Å
• c: 18.1656 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 18255.9 ± 0.3 ų
• Cell temperature: 83 ± 2 K
• Ambient diffraction temperature: 83 ± 2 K
• Number of distinct elements: 6
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0957
• Residual factor for significantly intense reflections: 0.0791
• Weighted residual factors for significantly intense reflections: 0.2134
• Weighted residual factors for all reflections included in the refinement: 0.2317
• Goodness-of-fit parameter for all reflections included in the refinement: 1.124
• Diffraction radiation wavelength: 0.78224 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No