Information card for entry 1556443

Structure parameters

• Formula: C22 H44 N4 Si4 Zn
• Calculated formula: C22 H44 N4 Si4 Zn
• SMILES: [Zn]1([n]2ccccc2c2[n]1cccc2)(N([Si](C)(C)C)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Reduction of 2,2'-Bipyridine by Quasi-Linear 3d-Metal(I) Silylamides-A Structural and Spectroscopic Study
• Authors of publication: Muller, I.; Schneider, C.; Pietzonka, C.; Kraus, F.; Werncke, C.G.
• Journal of publication: Inorganics
• Year of publication: 2019
• Journal volume: 7
• Pages of publication: 117
• a: 18.8806 ± 0.0012 Å
• b: 18.056 ± 0.0013 Å
• c: 17.6133 ± 0.0017 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6004.5 ± 0.8 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for significantly intense reflections: 0.07
• Weighted residual factors for all reflections included in the refinement: 0.0718
• Goodness-of-fit parameter for all reflections included in the refinement: 0.969
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No