Preparation and Molecular Structure of a Cyclopentyl-Substituted Cage Hexasilsesquioxane T6 (T = cyclopentyl-SiO1.5) Starting from the Corresponding Silanetriol
Authors of publication
Kahr, J.; Belaj, F.; Pietschnig, R.
Journal of publication
Inorganics
Year of publication
2017
Journal volume
5
Pages of publication
66
a
11.5359 ± 0.0016 Å
b
6.7079 ± 0.0009 Å
c
10.1493 ± 0.0013 Å
α
90°
β
115.83 ± 0.004°
γ
90°
Cell volume
706.9 ± 0.17 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0413
Residual factor for significantly intense reflections
0.0326
Weighted residual factors for significantly intense reflections
0.0829
Weighted residual factors for all reflections included in the refinement
0.0873
Goodness-of-fit parameter for all reflections included in the refinement
