Information card for entry 1556556

Structure parameters

• Formula: C36 H75 O9 P3 Pd3 Si3
• Calculated formula: C38.5 H75 O9 P3 Pd3 Si3
• Title of publication: Construction of a Planar Tetrapalladium Cluster by the Reaction of Palladium(0) Bis(isocyanide) with Cyclic Tetrasilane
• Authors of publication: Sunada, Y.; Taniyama, N.; Shimamoto, K.; Kyushin, S.; Nagashima, H.
• Journal of publication: Inorganics
• Year of publication: 2017
• Journal volume: 5
• Pages of publication: 84
• a: 11.2891 ± 0.0018 Å
• b: 12.711 ± 0.002 Å
• c: 19.549 ± 0.003 Å
• α: 81.516 ± 0.006°
• β: 85.854 ± 0.006°
• γ: 64.096 ± 0.005°
• Cell volume: 2495.6 ± 0.7 ų
• Cell temperature: 103 K
• Ambient diffraction temperature: 103 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0523
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for significantly intense reflections: 0.0774
• Weighted residual factors for all reflections included in the refinement: 0.083
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No