Information card for entry 1557046

Structure parameters

• Formula: C12 H35 Cl4 Cr2 N8 Na O18
• Calculated formula: C12 Cl4 Cr2 N8 Na O18.005
• Title of publication: Synthesis and Characterization of a Dinuclear Chromium(III) Complex with Two Amido Bridges and One Hydroxo Bridge. Crystal Structure of Na[(tacn)Cr(mu-NH2)2(mu-OH)Cr(tacn)](ClO4)4.H2O (tacn = 1,4,7-Triazacyclononane)
• Authors of publication: Andersen, Peter; Bengaard, Hanne; Glerup, Jorgen; Gumm, Andreas; Larsen, Sine
• Journal of publication: Acta Chemica Scandinavica
• Year of publication: 1998
• Journal volume: 52
• Pages of publication: 1313 - 1321
• a: 14.417 ± 0.002 Å
• b: 18.045 ± 0.002 Å
• c: 23.48 ± 0.003 Å
• α: 90°
• β: 90.244 ± 0.011°
• γ: 90°
• Cell volume: 6108.4 ± 1.3 ų
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.0894
• Weighted residual factors for significantly intense reflections: 0.1649
• Goodness-of-fit parameter for all reflections included in the refinement: 1.229
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No