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Information card for entry 1557094
Preview
Coordinates | 1557094.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C36 H90 Gd K N5 O6 Si6 |
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Calculated formula | C36 H90 Gd K N5 O6 Si6 |
SMILES | C[Si](C)(N([Gd](N([Si](C)(C)C)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C)[Si](C)(C)C)C.[K]1234567[O]8CC[O]1CC[N]21CC[O]3CC[O]4CC[N]5(CC8)CC[O]6CC[O]7CC1 |
Title of publication | The importance of the counter-cation in reductive rare-earth metal chemistry: 18-crown-6 instead of 2,2,2-cryptand allows isolation of [YII(NR2)3]1− and ynediolate and enediolate complexes from CO reactions |
Authors of publication | Ryan, Austin J.; Ziller, Joseph W.; Evans, William J. |
Journal of publication | Chemical Science |
Year of publication | 2020 |
Journal volume | 11 |
Journal issue | 7 |
Pages of publication | 2006 - 2014 |
a | 18.564 ± 0.003 Å |
b | 18.564 ± 0.003 Å |
c | 18.05 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 120° |
Cell volume | 5387 ± 1.5 Å3 |
Cell temperature | 88 ± 2 K |
Ambient diffraction temperature | 88 ± 2 K |
Number of distinct elements | 7 |
Space group number | 155 |
Hermann-Mauguin space group symbol | R 3 2 :H |
Hall space group symbol | R 3 2" |
Residual factor for all reflections | 0.0304 |
Residual factor for significantly intense reflections | 0.0235 |
Weighted residual factors for significantly intense reflections | 0.0411 |
Weighted residual factors for all reflections included in the refinement | 0.0426 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.005 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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