Crystallography Open Database

Information card for entry 1557551

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Coordinates	1557551.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C151 H208 Mg4 N12 O6
Calculated formula	C151 H208 Mg4 N12 O6
Title of publication	Sterically controlled reductive oligomerisations of CO by activated magnesium(i) compounds: deltate vs. ethenediolate formation
Authors of publication	Yuvaraj, K.; Douair, Iskander; Jones, Dafydd D. L.; Maron, Laurent; Jones, Cameron
Journal of publication	Chemical Science
Year of publication	2020
Journal volume	11
Journal issue	13
Pages of publication	3516 - 3522
a	17.919 ± 0.0006 Å
b	19.6004 ± 0.0009 Å
c	20.9467 ± 0.0007 Å
α	79.292 ± 0.003°
β	75.685 ± 0.003°
γ	86.86 ± 0.003°
Cell volume	7004 ± 0.5 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1648
Residual factor for significantly intense reflections	0.09
Weighted residual factors for significantly intense reflections	0.255
Weighted residual factors for all reflections included in the refinement	0.3129
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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